Brookfield DV2T Viscometer Manual do Utilizador Página 24

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Brookeld Engineering Labs., Inc. Page 24 Manual No. M13-167-B0614
Manysamplesmustbecontrolledtoaspecictemperatureforviscositymeasurement.
When conditioning a sample for temperature, be sure to temperature control the
containerandspindleaswellasthesample.
Pleaseseeourpublication,“MoreSolutionstoStickyProblems”,formoredetailrelating
to sample preparation.
III.3 Selecting a Spindle/Speed
TheDV2Thasthecapabilityofmeasuringviscosityoveranextremelywiderange.For
example,theDV2TRVcanmeasureuidswithintherangeof100-40,000,000cP.This
rangeisachievedthroughtheuseofseveralspindlesovermanyspeeds.SeeAppendix
B for details.
Theprocessofselectingaspindleandspeedforanunknownuidisnormallytrialand
error. An appropriate selection will result in measurements made between 10-100 on
the instrument % torque scale.Twogeneralruleswillhelpinthetrialanderrorprocess.
1)Viscosityrangeisinverselyproportionaltothesizeofthespindle.
2)Viscosityrangeisinverselyproportionaltotherotationalspeed.
Inotherwords:tomeasurehighviscosity,chooseasmallspindleand/oraslowspeed.
Ifthechosenspindle/speedresultsinareadingabove100%,thenreducethespeedor
chooseasmallerspindle.
Experimentationmayrevealthatseveralspindle/speedcombinationswillproducesatisfactory
resultsbetween10-100%.Whenthiscircumstanceoccurs,anyofthespindlesmaybe
selected.
Non-Newtonianuidbehaviorcanresultinthemeasuredviscosityandyieldstresschanging
ifthespindleand/orspeedischanged.Seeourpublication,“MoreSolutionstoSticky
Problems”,formoredetails.
When viscosity data must be compared, be sure to use
the same test methodology: namely the same instrument,
spindle, speed, container, temperature and test time.
DV2TLVViscometersareprovidedwithasetoffourspindles
andanarrowguardleg;DV2TRVViscometerscomewithaset
ofsixspindlesandawiderguardleg;DV2THAandDV2THB
Viscometerscomewithasetofsixspindlesandno guardleg.
(SeeAppendixGformoreinformationontheguardleg.)
The spindles are attached to the viscometer by screwing
themontothecouplingnutonthelowershaft(seeFigure
III-1).Notethatthespindleshavealeft-handthread.The
lowershaftshouldbesecuredandslightlyliftedwithonehand
whilescrewingthespindletotheleft.Thefaceofthespindle
nutandthematchingsurfaceonthelowershaftshouldbe
smoothandcleantopreventeccentricrotationofthespindle.
Spindlescanbeidentiedbythenumberonthesideofthe
spindle coupling nut.
The motor should be OFF whenever
spindlesarebeingremovedorattached.
Figure III-1
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Comentários a estes Manuais

Sachin Vaijanath Ashture 05 Mar 2025 | 15:48:33

It's good information