Brookfield DV2T Viscometer Manual do Utilizador Página 74

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Brookeld Engineering Labs., Inc. Page 74 Manual No. M13-167-B0614
BrookeldViscosityStandardFluidGeneralInformation
We recommendthat Brookeld Viscosity Standard Fluids be replaced on an annual
basis,oneyearfromdateofinitialuse.Theseuidsarepuresiliconeandarenotsubject
tochangeovertime.However,exposuretooutsidecontaminantsthroughnormaluse
requiresreplacementonanannualbasis.Contaminationmayoccurbytheintroduction
ofsolvent,standardofdifferentviscosityorotherforeignmaterial.
ViscosityStandardFluidsmaybestoredundernormallaboratoryconditions.Disposal
shouldbeinaccordancewithstate,localandfederalregulationsasspeciedonthe
materialsafetydatasheet.
BrookeldEngineeringLaboratoriesdoesnotrecertifyViscosityStandardFluids.Wewill
issueduplicatecopiesoftheCerticateofCalibrationforanyuidwithintwoyearsofthe
purchasedate.BrookeldViscosityStandardFluidsarereusableprovidedtheyarenot
contaminated.Normalpracticeforusageina600mLbeakeristoreturnthematerial
fromthebeakerbackintothebottle.Whenusingsmallervolumesinaccessoriessuch
asSmallSampleAdapter,ULAdapterorThermosel,theuidisnormallydiscarded.
CalibrationProcedureforLV#1-3(#61-63)andRV,HA,HB#1-6BrookeldSpindles
Please note that the LV #4 (64) and RV, HA, HB #7 (07) spindles have been omitted
fromthisprocedure.Brookelddoesnotrecommendtheuseofthesespindles
to perform a calibration check on your instrument. Reasons pertain to the small
amount of spindle surface that makes contact with the viscosity standard, the
difcultyofestablishingtheimmersionmarkpreciselyandtheneedforprecise
temperature control at 25°C in the immediate vicinity of the spindle.
Followthesestepsusingoneoftherecommendedspindlestoverifycalibrationonyour
instrument:
1) Placetheviscositystandarduid(inthepropercontainer)intothewaterbath.
2) Lower theDV2T into measurement position (with guard leg ifLV or RV series
Viscometerisused).
3) AttachthespindletotheViscometer.Ifyouareusingadisk-shapedspindle,avoid
trappingairbubblesbeneaththediskbyrstimmersingthespindleatanangle,
andthenconnectingittotheViscometer.
4) The viscosity standard uid, together with the spindle, should be immersed in
the bath for a minimum of 1 hour, stirring the uid periodically, prior to taking
measurements.
5) After1hour,checkthetemperatureoftheviscositystandarduidwithanaccurate
thermometer.
6) Iftheuidisattesttemperature(±0.1°Cofthespeciedtemperature,normally
25°C),measuretheviscosityandrecordtheViscometerreading.
Note: The spindle
must rotate at least ve (5) times before readings are taken.
7) TheviscosityreadingshouldequalthecPvalueontheuidstandardtowithinthe
combinedaccuraciesoftheViscometerandtheviscositystandard(asdiscussed
inthesection,attheendofthisAppendix,entitledInterpretationofCalibrationTest
Results)whichappearslaterinthissection.
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Comentários a estes Manuais

Sachin Vaijanath Ashture 05 Mar 2025 | 15:48:33

It's good information